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Abstract of the Ph. D. thesis of Paulo Guilherme Leandro de Oliveira

Isoenzyme Analysis for the Identification of Hybrids of Cork Oak and Holm Oak

University of Évora, Portugal

2006

Aims

In view of the persisting uncertainties on the hybrid origin of cork oak trees that produce the so-called "preguenta" cork, a question impossible to ignore in the recurring discussion over the mixed stands with cork oak and holm oak in Portugal, and in order to obtain credible estimates of the hybridization rates in these stands, the present study aimed at establishing genetic criteria for the discrimination between the two species and their hybrids.

Framework and Approach

This study was part of the PAMAF Project 8153 (Instituto Nacional de Investigação Agrária) approved in 1997, coordinated by Prof. Carola Meierrose, of the Biology Department, University of Évora, in which the University of Évora, the National Forestry Station (Estação Florestal Nacional) and the Regional Office for Agriculture in Alentejo (Direcção Regional de Agricultura do Alentejo) took part. The option taken was to analyse enzymatic markers, under the hypothesis that interspecific variations in some of them would be diagnostic between the two species and their hybrids, in part because isoenzymes are very suitable for large-scale screenings, and also because at the time practically no DNA analysis was made on cork oak, not even internationally.

Sampling

To monitor the occurrence of new hybrids, three mixed stands were selected and in 1998 acorns were collected from trees of both species, which were sown and raised in a nursery. The same was done in reference stands ("pure", either of cork or holm oak) located at distances from the other species that would a priori preclude any contact. The seedlings that were obtained made for most of the analysed material, the remainder including the adults from the mixed stands, to detect possible hybridization within that generation and, through the verification of the genotypes in the progenies, to confirm the kinship, important because the acorns were collected on the ground. Thus each adult within the mixed stands was marked and numbered. Finally, another reference were the hybrids themselves, and the project set out to make an inventory of them, while sampling the progenies from some of them.

Integration with studies on flowering

The same project coupled isoenzyme analysis with records of flowering and fruiting on the adults. It was assumed that the opportunity for hybridization to occur increases with a higher overlap between the flowering time spans of each species each year. Holm oaks precede cork oaks by a few weeks, but this separation is only between average dates, is variable from year to year, for example in response to different temperature profiles, and is of little practical significance because of the large intraspecific scatter among individuals, in their flowering timings, in both species. Hence, marking the adults in each mixed stand also allowed monitoring the phenology of flowering in each individual for the year of 1998, for the event that, based on the timing proximity of one tree with those of the other species, its progeny could be considered more or less likely to contain hybrids.

Specific component of this study

This thesis refers mainly to the isoenzyme analysis component of the project. With a methodological implementation projecting a future capacity for processing large samples, genetic markers were defined for the discrimination between cork oak and holm oak, and their hybrids, and their analysis among the progenies, beyond the purpose of detecting hybrids, also allowed the preliminary characterization of the biology of reproduction in the two species and the hybrids.

Results

Enzyme markers analysed

Most of the enzyme activities tested in leaf extracts from cork oak or holm oak produced some signal in at least one separation system, but only a minority (11 in 35) were considered consistent. Of the remainder, 9 gave good results in one single attempt and might be confirmed on future trials. In seed extracts the results were essentially the same as those in leaves, but at least 1 was consistent only in the former. Some activities were detected only in leaves from other species of dicotyledons, but not in those from species of Quercus, thus excluding that the extraction method in itself caused a failure in detecting them.

There were 8 enzyme activities that, after routine analysis in leaf extracts and seeds from the reference and mixed stands, and hybrids, could contribute for the dircrimination between cork oak, holm oak and their hybrids: diaphorase (DIA), malate dehydrogenase (MDH), glutathione reductase (GsR), phosphoglucomutase (PGM), 6-phosphogluconate dehydrogenase (PGD), 6-phosphoglucose isomerase (PGI) and esterases (EST).

Other activities appear to show the same potential, but are yet to be confirmed under routine analyses: high isoelectric point esterases (EST) and fluorogenic acid phosphatases (ACP-F), and in seeds only, L-glutamate dehydrogenase (GDH).

Genetic interpretations for the polymorphisms in DIA, GsR, PGM, PGI and (partly) MDH) were achieved.

Applications of the enzyme markers electrophoretic analysis

From the routine analyses primarily designed for the validation of discriminant markers and the detection of hybrids, it was possible to:

Confirm the detected interspecific, and part of the intraspecific, contaminants; partially characterise 9 hybrids, one among them (SM2) possibly the product of a backcross between a hybrid and a cork oak; in the absence of hybrids in the mixed stands progenies of 1998, compute a high boundary for the relevant probability of hybridization, for which the most conservative estimate is P < 0,043%; characterise adults and seedlings with atypical phenotypes, the number of which appears to be very low; characterise samples from 45 "preguenta" cork trees, with two markers (DIA and PER) giving signs of possible introgression of holm oak genes in some of them; quantify the specificity and sensitivity of each marker, used in the routine analyses, for distinguishing hybrids and holm oaks from cork oak; determine the pollen origin for each seedling from the hybrids SM1, SM2 and SES; analyse the intraspecific frequencies at the loci Pgm (holm oak) and Pgi-B (cork oak), thus showing the ability to treat the three mixed stands as one population, in each species, and the computation of various population genetic estimators; reveal disparities between the distribution frequencies in pollen, female gametophytes and seedlings, especially at Pgm, allowing the estimation of neutral values for Ne in the order of 5 to 7 in both species; estimate the percentage of unrelated pollen at 81% in holm oak (Pgm) and 84% in cork oak (Pgi-B).

The analysis of cork oak seedlings from provenances of the 7 countries spanning the species range has not revealed any isoenzyme pattern contradicting the specificity of the hybridization markers defined on the basis of the reference stands (Santiago do Cacém, Azeiteiros and Testa) and mixed stands (Mitra, Feijoas do Ramos and Alfaiates).

The application of the same extraction protocol to other species in the order Fagales showed a more or less striking variation of the isoezyme patterns between taxonomic levels (variably according to the activities) and confirmed the potential of application of these markers to discrimination work between other taxa.

Discussion

Progress accomplished

The present work contains the following progress in the initially proposed research:

1. Discovery and validation of isoenzyme markers for the distinction between cork oak and hybrids and their descendants;

2. Confirmation, with genetic markers, of the hybrid status of the trees known as "cerqueiro" oaks;

3. Estimate of a very low hybridization rate (less than 0.1%) in the mixed stands studied;

4. Detection, in cork oak as well as in holm oak, of markers of introgression from the other species;

5. Preliminary analysis of cork oaks that produce "preguenta" cork;

6. Preliminary analysis of hybrid progenies, including the demonstration that pollen grains from either of the two parental species are involved, as well as a relatively high selfing rate;

7. Preliminary analysis of the allelic frequencies in two marker loci, one of each species, and derivation of a relatively low neutral value of Ne;

8. Demonstration of the same methodology in other species of the genus Quercus and related taxa.

Genetic demonstration of the "cerqueiro" oaks hybrid character

The hybrid status of the "cerqueiro" oaks was verified based on genetic markers (isoenzymes), thus contributing to establish these markers as efficient means to detect hybrids between cork oak and holm oak. The fact that this approach is feasible on leaf material removes limitations that might be posed by age or season.

Fertility of the "cerqueiro" hybrids and production of recombinants

Knowing the heredity for the discriminating isoenzymes, although with some limtations, allowed the identification in the progenies of 3 hybrids of the type of pollen from which each descendant derived, and from that the realization that the hybrids are fertile with pollen either of cork oak, holm oak or hybrids, the latter to a proportion apparently very high for what is expected in Quercus.

Although inefficient, because of the small number of markers, to verify the conjecture of introgressed holm oak genes in the "preguenta"-producing cork oak trees, the results from a limited sampling of such trees, along with demonstration of fertility of these hybrids with cork oak, favour this conjecture.

Incidence of hybridization

The absence of hybrids among the progenies from cork and holm oaks in the mixed stands allowed only the calculation of a high boundary for their actual incidence, estimated at very low values. The biology of reproduction of both species, based on the evidence from intraspecific polymorphic markers, leads to postulate that, along with the a priori relevant factor for hybridization that topographic proximity between individuals of the two species must be, an overlap of flowering times must also exist but is not sufficient; the individual compatibility between mating trees must also play some role. Therefore, the incidence of hybridization is predicted to be very low, but it might occur at higher rates in foci where for several years all these factors coincide. The frequency at which it is said that another type of cork oak called "negral" occurs in Alentejo is not compatible with the estimates made, hence it is supposed that this designation is not for real hybrids.

Future applications

The present study allows to envisage several lines of investigation, where the enzyme markers used in large scale in the present study, and others that in the meantime are proven useful, will play a relevant role. The verification of the incidence of hybridization in mixed stands, based on a sampling spanning several years and encompassing different provenances, the study of the hybrids in their biology of reproduction, and of the ritidome development in their recombinant progenies, are very interdependent. The isoenzyme markers can be also of great use in the research on the presumed holm oak introgression in cork oak trees that produce "preguenta" cork and in the "negral" type.

University of Évora, on November 2006